HomeMy WebLinkAbout22-102032-UP Lead and Arsenic Sampling Report (ASRCO)-5-4-22
214 EAST GALER STREET, SUITE 3 00, SEATTLE, WA 98102 206.233.9639 MAIN 866.727.0140 FAX PBSUSA.COM
October 8, 2021
Federal Way Public Schools Capital Projects
1211 S 232nd St
Federal Way, WA 98004
Email: fwpscp18@fwps.org
RE: Illahee Middle School – Arsenic and Lead Soil Sampling
36001 1st Avenue South, Federal Way, Washington PBS Project #41519.009
Federal Way Public Schools (FWPS) contracted PBS Engineering and Environmental Inc. (PBS) to evaluate the
potential for arsenic and lead contaminants in near-surface soils at the site of Illahee Middle School (IMS) prior to
site redevelopment as part of the Illahee Middle School Replacement Project.
On August 11, 2021, PBS performed soil sampling activities to determine the levels of arsenic and lead in shallow
soil at IMS in Federal Way, Washington (Figure 1). This report presents the findings of the sampling activities and
provides recommendations for regulatory compliance as well as for the handling and management of impacted
soils during future redevelopment. The scope of services was presented in the Proposal to Provide a Hazardous Materials Survey and Soil Sampling (WA31520R1) by PBS, dated July 6, 2021. BACKGROUND
IMS is located within the widespread soil contamination plume of the former Asarco smelter operation. The
Asarco Company operated a copper smelter in Tacoma from 1890 to 1985. Smelter operations emitted an
airborne plume of particulates with arsenic, lead, and other heavy metals that were distributed over a wide region
of the Puget Sound. As a result, these metals have been found in near surface soils at concentrations which may
pose a threat to human health and/or the environment.
Ecology’s Tacoma Smelter Plume Model Remedies Guidance (Smelter Plume Guidance) recommends soil sampling
at properties in areas with estimated arsenic levels above the state cleanup level of 20 parts per million (ppm)1.
Ecology’s Dirt Alert website 2 maps the site within an area of predicted arsenic concentrations of less than 20ppm. However, FWPS requested characterization of soils following the Smelter Plume Guidance in a conservative effort
to prevent exposure. Based on the predicted arsenic concentration at the site and the approximate 28.9-acre area
of the parcel, the Smelter Plume Guidance recommends samples be collected from a minimum of 67 locations. REGULATORY CRITERIA
Per the Smelter Plume Guidance “if arsenic or lead levels are elevated for any decision unit on the property, that decision unit needs cleanup.” Elevated is defined as:
• Average arsenic > 20 ppm, equivalent to milligrams per kilogram (mg/kg) or average lead > 250 ppm; or
• Maximum (any one sample) arsenic > 40 ppm or maximum lead > 500 ppm.
1 “Tacoma Smelter Plume Model Remedies Guidance: Sampling and cleanup of arsenic and lead contaminated soils”, Washington State Department of Ecology, July 2019, Publication No. 19-09-101
2 https://apps.ecology.wa.gov/dirtalert/
Federal Way Public Schools Illahee Middle School Arsenic and Lead Sampling Report October 8, 2021 Page 2
41519.009
Ecology’s Model Toxics Control Act (MTCA) has established cleanup levels for arsenic and lead for unrestricted land use that are protective of human health and the environment 3. Ecology’s MTCA Method A cleanup levels
(CULs) for unrestricted land use for arsenic and lead are applicable for comparison to any single soil sample
concentration. The CULs for arsenic and lead are presented below:
• The CUL for arsenic is 20 milligrams per kilogram (mg/kg)
• The CUL for lead is 250 mg/kg.
CHARACTERIZATION SOIL SAMPLING
On August 11, 2021, eighty-four (84) discrete soil samples were collected from sixty-seven (67) locations around
the building landscaping and playfields of IMS. Following Ecology guidance, the property was divided into six
decision units based on past/current use as playfield or landscaped area. Decision units and sample locations are
shown on Figure 2. A summary of the decision units is provided below. The number of samples collected for
analysis per decision unit for this project is based on the Smelter Plume Guidance.
Decision Units
Decision
Unit ID
Soil disturbance
planned?
Number of samples
collected (0-6”)
Number of samples collected
(6-12”)
Acres
(approximate)
Total Number
of Samples
1 unknown 15 3 6.71 18
2 unknown 7 2 3.22 9
3 unknown 24 7 10.3 31
4 unknown 6 2 2.20 8
5 unknown 7 1 3.00 8
6 unknown 8 2 3.67 10
0-6” = Soil samples were collected from the 0-6 inch depth interval 6-12” = Soil samples were collected from the 6-12 inch depth interval Per the Smelter Plume Guidance, one (1) discrete sample was collected at each sample location from a depth
interval of 0 to 6 inches below ground surface (bgs). A second discrete sample was collected at every fourth
location from a depth interval of 6 to 12 inches bgs. Sample locations were chosen in a manner that maximized
coverage of the decision units and did not contain areas with surface cover or buildings at the time of sample
collection.
Soil sample collection started just below any surface cover layer (e.g., sod or grass). A hand spade and a hand
auger were used to complete 6-inch deep test holes. A soil sample was collected at a depth of less than 6 inches
below ground surface at each location. At every fourth location, upon collection of the 0- to 6-inch sample, the
hole was advanced to a depth of 12 inches, and a second sample was collected from the 6- to 12-inch depth
interval using the same methods described above. PBS personnel wore disposable nitrile gloves to protect against cross-contamination between samples. Soil retained for analysis was packed into laboratory-provided containers, labeled and transported on ice under chain
3 “Model Toxics Control Act Regulation and Statute”, Washington State Department of Ecology, 2013 Revision, Publication No. 94-06
Federal Way Public Schools Illahee Middle School Arsenic and Lead Sampling Report October 8, 2021 Page 3
41519.009
of custody documentation to Friedman and Bruya, Inc. in Seattle, an Ecology accredited analytical laboratory.
Samples were analyzed for total arsenic and lead using EPA Method 6020. Total arsenic and lead results were
reported on a dry weight basis. ANALYTICAL RESULTS
Analytical results from soil samples collected on site are below MTCA Method A CULs for arsenic, except for one
(1) sample from a single location (Sample ID: DU-4-3) in the western side of Decision Unit 4 adjacent to 361st Place
(see Figure 2). The sample collected from 0 to 6 inches bgs at location DU-4-3 contained arsenic at a
concentration of 28.6 mg/kg. The concentration is in exceedance of the CUL but is not considered elevated per
the Smelter Plume Guidance.
Analytical results for lead from soil samples collected on-site are below the MTCA Method A cleanup level of 250
mg/kg.
Based on the analytical results of soil samples collected on-site, average arsenic and lead concentrations were
calculated for each decision unit and are presented below.
Average Concentrations per Decision Unit
Decision Unit ID Mean Concentration (0-6”) Mean Concentration (6-12”)
As Pb As Pb
1 7.43 14.0 4.21 8.37
2 7.56 17.2 4.22 7.59
3 2.20 4.36 3.65 7.13
4 2.86 3.54 2.19 6.78
5 4.21 8.37 2.56 7.21
6 4.22 7.59 3.28 4.58
MTCA A Cleanup Level 20 250 20 250
(0-6”) (Pb / As) = Average Concentration at the 0 to 6-inch interval for arsenic (As) and lead (Pb) in mg/kg
(6-12”) (Pb / As) = Average Concentration at the 6 to 12-inch interval for arsenic (As) and lead (Pb) in mg/kg
Analytical results from soil samples collected on-site are summarized in Table 1. Figure 2 depicts the decision unit
boundaries and the locations where analytical results indicated lead or arsenic concentrations above MTCA
Method A CULs. Laboratory reports are provided in Attachment A.
Federal Way Public Schools Illahee Middle School Arsenic and Lead Sampling Report October 8, 2021 Page 4
41519.009
CONCLUSIONS
Based on the analytical results of the soil sampling, and using Ecology’s Tacoma Smelter Plume Model Remedy
Guidance, June 2019 (Guidance), the following conclusions and recommendations were made regarding the
handling and management of project site soils.
Decision Unit 1
No further action is advised within Decision Unit 1 based on the results of soil sampling conducted on August 11,
2021.
Decision Unit 2
No further action is advised within Decision Unit 2 based on the results of soil sampling conducted on August 11,
2021.
Decision Unit 3
No further action is advised within Decision Unit 3 based on the results of soil sampling conducted on August 11,
2021.
Decision Unit 4
Analytical results from the discrete soil sample collected at sample location DU-4-3 indicated arsenic
concentrations are above the MTCA Method A CUL in the top 6” bgs. A deeper sample was not collected in this
location. However, the average concentration of arsenic detected in samples taken at this depth from this decision
unit is 2.86 mg/kg, which is not considered “elevated” per the Guidance. Therefore, no cleanup is required in this
decision unit and no further action is advised based on the results of soil sampling conducted on September 11,
2021.
Decision Unit 5
No further action is advised within Decision Unit 5 based on the results of soil sampling conducted on August 11,
2021.
Decision Unit 6
No further action is advised within Decision Unit 6 based on the results of soil sampling conducted on August 11,
2021.
Federal Way Public Schools Illahee Middle School Arsenic and Lead Sampling Report October 8, 2021 Page 5
41519.009
LIMITATIONS
This investigation was conducted to characterize lead and arsenic distributions in shallow soils on-site, with a
focus on protection of human health and the environment. The data collected in this investigation are not
intended for the purposes of waste profiling for offsite disposal, or for estimation of volume or tonnage of soil
requiring disposal.
PBS has prepared this report for use by FWPS. This report is not intended for use by others without the written
consent of the FWPS. Our interpretation of soil conditions in this study was based on field observations and
analytical data from the indicated explorations. Regulated substances may exist in portions of the site that were
not explored or analyzed. The conclusions in this report are not to be considered a legal opinion as the client’s
duty concerning due diligence relating to potential liabilities in leasing, owning, or purchasing real estate.
PBS ENGINEERING AND ENVIRONMENTAL INC.
Nathan Dickey, LG Project Geologist
Reviewed By:
James Welles, LHG
Project Geologist
Attachments:
Figure 1: Vicinity Map
Figure 2: Sample Location Map
Table 1: Laboratory Data Summary Table
Attachment A: Laboratory Data
Figures
FIGURE1
Lots 64-78
SOURCES: USGS NATIONAL MAP, 2020PROJECTION: NAD 2011 WA STATE PLANE NORTH LAMBERT US FT
PREPARED FOR: FEDERA L WA Y PUBLIC SC HOO LS
SITE VICINIT Y
0 2,000 4,0001,000 Feet
1 " = 2,000 feet
\\pbsenv.lan\L\Projects\41000\41519 Federal Way Public Schools\41519.009 Illahee Middle School\GIS\Fig1_SiteVicinity.mxd; AUTHOR: NathanDOCT 202141519.010
oSCALE: OLYMPIA
SPOKANE
PROJECT
LOCATION
SEATTLE SPOKANE
ILLAHEE M IDDLE SCHO OL36001 1ST AVE S, FEDERAL WAY, WASHINGTON
PROJECTLOCATION
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DU-2-2
DU-2-1
DU-2-5
DU-2-7
DU-2-6
DU-2-3
DU-2-4
DU-3-1
DU-3-2
DU-3-3 DU-3-6
DU-3-5DU-3-4
DU-3-7DU-3-8
DU-3-9DU-3-10
DU-3-11
DU-3-12
DU-3-13
DU-3-19
DU-3-18
DU-3-17
DU-3-16DU-3-15
DU-3-14
DU-5-2
DU-5-1
DU-5-4
DU-5-5
DU-5-6
DU-5-7
DU-5-3
DU-6-5 DU-6-6
DU-6-4
DU-6-3
DU-6-8
DU-6-7
DU-6-2DU-6-1
DU-3-21
DU-3-20
DU-3-22
DU-3-23
DU-3-24
DU-4-5DU-4-4
DU-4-3
DU-4-2
DU-4-1 DU-4-6
DU-1-4
DU-1-8
DU-1-3
DU-1-7
DU-1-11
DU-1-15
DU-1-14
DU-1-13DU-1-12
DU-1-10DU-1-9
DU-1-6DU-1-5
DU-1-2DU-1-1
DU-1
DU-2
DU-3
DU-5
DU-6
DU-4
O PROJECT
DATEOCT 2021
41519.010
FIGURESOIL SAMPLE LOCATIONS0 150 30075'
PREPARED FOR: FEDERAL WAY PUBLIC SCHOOLSIMAGERY SOURCE: PBS UAS AERIAL PHOTOGRAPHY, AUGUST 11, 2021; ESRI AERIAL IMAGERY (SURROUNDINGS)PROJECTION: NAD 2011 WA STATE PLANE NORTH LAMBERT US FT
\\pbsenv.lan\L\Projects\41000\41519 Federal Way Public Schools\41519.009 Illahee Middle School\GIS\Fig2_SoilSamplingLocations.mxd; AUTHOR: NathanD1 inch = 150 feet PBS Engineering and Environmental Inc.pbsusa.com214 E Galer Street, Suite 300Seattle, WA 98102206.233.9639ILLAHEE MIDDLE SCHOOL36001 1ST AVE S, FEDERAL WAY, WASHINGTONLEGEND
Sur face Soil Sample Locationand Name
!
Sample taken from 0-6 inchesbelow ground surface;Total arsenic < 20 mg/kg;Total lead < 250 mg/kg
G
Samples taken from 0-12inches below ground surface;Total arsenic < 20 mg/kg;Total lead < 250 mg/kg
!(Total Arsenic: 20 - 40 mg/kg;Total lead < 250 mg/kg
FULL SIZE SHEET FORMAT IS 11X17: IF PRINTED SIZE IS NOT 11X17, THEN THIS SHEET FORMAT HAS BEEN MODIFIED AND INDICATED DRAWING SCALE IS NOT ACCURATE
(Rotation: 2° W)
2
Notes:1. Samples analyzed for Total Lead and Total Arsenic via EPA Method 6020.2. The detected concentration of arsenic exceeded the Washington State Department of Ecology Model Toxics Control Act Method A Cleanup Levels for Unrestricted Land Use.at one location (DU-4-3).3. mg/kg is milligrams per kilogram.AND DECISION UNITS
Table
TABLE 1
SOIL ANALYTICAL RESULTS
Illahee Middle School
36001 1st Avenue South, Federal Way, Washington
PBS Project No. 41519.009
Arsenic Lead Notes:
MTCA Method A - Soila 20 250
"Elevated" Concentrationb 40 500
1 0-6 5.49 12.2
2 0-6 7.70 19.8
3 0-6 15.0 28.5
4 0-6 7.58 33.8
5 0-6 6.96 18.3 Abbreviations & Acronyms:
6 0-6 4.65 8.84 mg/kg - milligrams per kilogram
7 0-6 9.20 18.8 bgs - below ground surface
8 0-6 12.4 19.0
9 0-6 8.58 10.6 Footnotes:
10 0-6 7.07 7.51
11 0-6 3.63 4.31
12 0-6 4.74 4.35
13 0-6 8.80 11.8
14 0-6 6.17 4.56
15 0-6 3.45 6.89
7.43 14.0
4 6-12 7.56 17.2
12 6-12 2.20 4.36
15 6-12 2.86 3.54
4.21 8.37
1 0-6 4.22 7.59
2 0-6 3.65 7.13
3 0-6 2.19 6.78
4 0-6 2.56 7.21
5 0-6 3.28 4.58
6 0-6 1.98 6.22
7 0-6 2.04 6.52
2.85 6.58
1 6-12 3.58 5.06
5 6-12 2.51 3.99
3.05 4.53
1 0-6 4.37 15.3
2 0-6 4.01 8.78
3 0-6 4.25 9.59
4 0-6 4.85 10.8
5 0-6 6.24 11.6
6 0-6 3.56 7.55
7 0-6 3.37 7.41
8 0-6 2.72 4.52
9 0-6 15.2 28.6
10 0-6 10.9 20.9
11 0-6 8.67 18.6
12 0-6 10.9 18.9
13 0-6 12.0 23.6
14 0-6 2.75 7.54
15 0-6 7.69 24.1
16 0-6 8.82 15.2
17 0-6 5.10 10.2
18 0-6 13.6 18.4
19 0-6 10.8 20.5
20 0-6 4.84 11.4
21 0-6 8.99 18.8
22 0-6 9.46 19.3
23 0-6 6.86 26.5
24 0-6 8.05 14.9
7.42 15.5
2 6-12 4.72 9.78
7 6-12 3.74 8.26
9 6-12 14.8 35.7
10 6-12 5.21 8.76
14 6-12 7.98 23.3
17 6-12 3.77 4.75
22 6-12 9.46 18.2
7.10 15.5
3
Average (0 to 6 inches bgs)
Average (6 to 12 inches bgs)
1
Average (0 to 6 inches bgs)
Average (6 to 12 inches bgs)
2
Average (0 to 6 inches bgs)
Average (6 to 12 inches bgs)
a Washington State Department of
Ecology Model Toxics Control Act
Method A Cleanup Level for Unrestricted
Land Use as established in WAC 173-340-
900.
b Washington State Department of
Ecology Tacoma Smelter Plume Model
Remedies Guidance, "Sampling and
Cleanup of Arsenic and Lead
Contaminated Soils", Publication
Number 19-09-101, July 2019.
Bold and italicized indicates detected
concentration is defined as elevated Per
Smelter Plume Guidance.
Bold indicates detected concentration
exceeds MTCA Method A Cleanup Level
Decision
Unit
Location Sample Depth Range
(inches bgs)
Metals (mg/kg)
Adopted
Criteria
1 of 2
TABLE 1
SOIL ANALYTICAL RESULTS
Illahee Middle School
36001 1st Avenue South, Federal Way, Washington
PBS Project No. 41519.009
Arsenic Lead Notes:
MTCA Method A - Soila 20 250
"Elevated" Concentrationb 40 500
Bold indicates detected concentration
exceeds MTCA Method A Cleanup Level
Decision
Unit
Location Sample Depth Range
(inches bgs)
Metals (mg/kg)
Adopted
Criteria
1 0-6 10.4 21.3
2 0-6 10.4 34.4
3 0-6 28.6 43.0
4 0-6 2.73 8.10
5 0-6 4.81 29.8
6 0-6 9.79 20.1
11.1 26.1
4 6-12 2.50 4.95
6 6-12 12.9 20.9
7.70 12.9
1 0-6 5.14 12.2
2 0-6 4.36 10.7
3 0-6 2.14 2.77
4 0-6 3.15 5.44
5 0-6 2.61 5.40
6 0-6 2.32 5.80
7 0-6 2.47 5.82
3.17 6.88
4 6-12 2.26 3.63
2.26 3.63
1 0-6 2.16 3.26
2 0-6 1.60 2.69
3 0-6 2.12 2.89
4 0-6 2.29 3.79
5 0-6 1.46 2.90
6 0-6 1.87 2.69
7 0-6 3.60 7.42
8 0-6 3.54 10.4
2.33 4.51
3 6-12 1.95 2.78
7 6-12 3.05 4.94
2.50 3.86
Bold and italicized indicates detected
concentration is defined as elevated Per
Smelter Plume Guidance.
Average Concentration of All Site Samples 4.86 9.11
4
Average (0 to 6 inches bgs)
Average (6 to 12 inches bgs)
5
Average (0 to 6 inches bgs)
Average (6 to 12 inches bgs)
6
Average (0 to 6 inches bgs)
Average (6 to 12 inches bgs)
2 of 2
Attachment A
Laboratory Report and Chain of Custody Documentation
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
James E. Bruya, Ph.D. 3012 16th Avenue West
Yelena Aravkina, M.S. Seattle, WA 98119-2029
Michael Erdahl, B.S. (206) 285-8282
Arina Podnozova, B.S. fbi@isomedia.com
Eric Young, B.S. www.friedmanandbruya.com
August 23, 2021
Nathan Dickey, Project Manager
PBS Engineering and Environmental, Inc.
214 E. Galer St, Suite 300
Seattle, WA 98102
Dear Mr Dickey:
Included are the results from the testing of material submitted on August 16, 2021
from the Illahee MS Soil Sampling 41515.009, F&BI 108248 project. There are 98
pages included in this report. Any samples that may remain are currently scheduled
for disposal in 30 days, or as directed by the Chain of Custody document. If you would
like us to return your samples or arrange for long term storage at our offices, please
contact us as soon as possible.
We appreciate this opportunity to be of service to you and hope you will call if you
should have any questions.
Sincerely,
FRIEDMAN & BRUYA, INC.
Michael Erdahl
Project Manager
Enclosures
PBS0823R.DOC
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
1
CASE NARRATIVE
This case narrative encompasses samples received on August 16, 2021 by Friedman &
Bruya, Inc. from the PBS Engineering and Environmental Illahee MS Soil Sampling
41515.009, F&BI 108248 project. Samples were logged in under the laboratory ID’s
listed below.
Laboratory ID PBS Engineering and Environmental
108248 -01 DU3-23-6
108248 -02 DU3-24-6
108248 -03 DU3-9-6
108248 -04 DU3-9-12
108248 -05 DU3-8-6
108248 -06 DU3-5-6
108248 -07 DU3-4-6
108248 -08 DU3-2-6
108248 -09 DU3-2-12
108248 -10 DU3-3-6
108248 -11 DU3-1-6
108248 -12 DU3-6-6
108248 -13 DU3-7-6
108248 -14 DU3-7-12
108248 -15 DU3-10-6
108248 -16 DU3-10-12
108248 -17 DU3-11-6
108248 -18 DU3-12-6
108248 -19 DU3-13-6
108248 -20 DU3-16-6
108248 -21 DU3-14-6
108248 -22 DU3-14-12
108248 -23 DU3-15-6
108248 -24 DU3-17-6
108248 -25 DU3-18-6
108248 -26 DU3-17-12
108248 -27 DU3-19-6
108248 -28 DU3-20-6
108248 -29 DU3-21-6
108248 -30 DU3-22-6
108248 -31 DU3-22-12
108248 -32 DU4-5-6
108248 -33 DU4-4-6
108248 -34 DU4-4-12
108248 -35 DU4-3-6
108248 -36 DU4-2-6
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
2
CASE NARRATIVE (continued)
Laboratory ID PBS Engineering and Environmental
108248 -37 DU4-1-6
108248 -38 DU4-6-6
108248 -39 DU4-6-12
108248 -40 DU6-1-6
108248 -41 DU6-2-6
108248 -42 DU6-3-6
108248 -43 DU6-3-12
108248 -44 DU6-4-6
108248 -45 DU6-5-6
108248 -46 DU6-6-6
108248 -47 DU6-7-6
108248 -48 DU6-7-12
108248 -49 DU6-8-6
108248 -50 DU5-1-6
108248 -51 DU5-2-6
108248 -52 DU5-3-6
108248 -53 DU5-4-12
108248 -54 DU5-5-6
108248 -55 DU5-6-6
108248 -56 DU5-7-6
108248 -57 DU5-4-6
108248 -58 DU2-1-6
108248 -59 DU2-1-12
108248 -60 DU2-2-6
108248 -61 DU2-3-6
108248 -62 DU2-4-6
108248 -63 DU2-5-6
108248 -64 DU2-5-12
108248 -65 DU2-6-6
108248 -66 DU2-7-6
108248 -67 DU1-1-6
108248 -68 DU1-2-6
108248 -69 DU1-3-6
108248 -70 DU1-4-6
108248 -71 DU1-4-12
108248 -72 DU1-5-6
108248 -73 DU1-6-6
108248 -74 DU1-7-6
108248 -75 DU1-8-6
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
3
CASE NARRATIVE (continued)
Laboratory ID PBS Engineering and Environmental
108248 -76 DU1-9-6
108248 -77 DU1-10-6
108248 -78 DU1-11-6
108248 -79 DU1-12-6
108248 -80 DU1-12-12
108248 -81 DU1-13-6
108248 -82 DU1-19-6
108248 -83 DU1-15-6
108248 -84 DU1-15-12
All quality control requirements were acceptable.
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
4
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-23-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-01
Date Analyzed: 08/18/21 Data File: 108248-01.051
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 6.86
Lead 26.5
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
5
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-24-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-02
Date Analyzed: 08/18/21 Data File: 108248-02.091
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 8.05
Lead 14.9
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
6
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-9-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-03
Date Analyzed: 08/18/21 Data File: 108248-03.092
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 15.2
Lead 28.6
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
7
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-9-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-04
Date Analyzed: 08/18/21 Data File: 108248-04.093
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 14.8
Lead 35.7
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
8
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-8-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-05
Date Analyzed: 08/18/21 Data File: 108248-05.094
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.72
Lead 4.52
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
9
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-5-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-06
Date Analyzed: 08/18/21 Data File: 108248-06.099
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 6.24
Lead 11.6
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
10
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-4-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-07
Date Analyzed: 08/18/21 Data File: 108248-07.100
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.85
Lead 10.8
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
11
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-2-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-08
Date Analyzed: 08/18/21 Data File: 108248-08.101
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.01
Lead 8.78
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
12
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-2-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-09
Date Analyzed: 08/18/21 Data File: 108248-09.102
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.72
Lead 9.78
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
13
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-3-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-10
Date Analyzed: 08/18/21 Data File: 108248-10.103
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.25
Lead 9.59
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
14
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-1-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-11
Date Analyzed: 08/18/21 Data File: 108248-11.104
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.37
Lead 15.3
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
15
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-6-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-12
Date Analyzed: 08/18/21 Data File: 108248-12.105
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.56
Lead 7.55
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
16
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-7-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-13
Date Analyzed: 08/18/21 Data File: 108248-13.106
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.37
Lead 7.41
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
17
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-7-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-14
Date Analyzed: 08/18/21 Data File: 108248-14.110
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.74
Lead 8.26
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
18
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-10-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-15
Date Analyzed: 08/18/21 Data File: 108248-15.111
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 10.9
Lead 20.9
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
19
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-10-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-16
Date Analyzed: 08/18/21 Data File: 108248-16.112
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 5.21
Lead 8.76
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
20
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-11-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-17
Date Analyzed: 08/18/21 Data File: 108248-17.113
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 8.67
Lead 18.6
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
21
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-12-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-18
Date Analyzed: 08/18/21 Data File: 108248-18.114
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 10.9
Lead 18.9
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
22
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-13-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-19
Date Analyzed: 08/18/21 Data File: 108248-19.115
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 12.0
Lead 23.6
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
23
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-16-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-20
Date Analyzed: 08/18/21 Data File: 108248-20.116
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 8.82
Lead 15.2
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
24
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-14-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-21
Date Analyzed: 08/18/21 Data File: 108248-21.122
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.75
Lead 7.54
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
25
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-14-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-22
Date Analyzed: 08/18/21 Data File: 108248-22.117
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 7.98
Lead 23.3
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
26
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-15-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-23
Date Analyzed: 08/18/21 Data File: 108248-23.118
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 7.69
Lead 24.1
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
27
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-17-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-24
Date Analyzed: 08/18/21 Data File: 108248-24.125
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 5.10
Lead 10.2
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
28
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-18-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-25
Date Analyzed: 08/18/21 Data File: 108248-25.126
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 13.6
Lead 18.4
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
29
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-17-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-26
Date Analyzed: 08/18/21 Data File: 108248-26.127
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.77
Lead 4.75
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
30
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-19-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-27
Date Analyzed: 08/18/21 Data File: 108248-27.128
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 10.8
Lead 20.5
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
31
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-20-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-28
Date Analyzed: 08/18/21 Data File: 108248-28.129
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.84
Lead 11.4
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
32
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-21-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-29
Date Analyzed: 08/18/21 Data File: 108248-29.130
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 8.99
Lead 18.8
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
33
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-22-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-30
Date Analyzed: 08/18/21 Data File: 108248-30.134
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 9.46
Lead 19.3
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
34
Analysis For Total Metals By EPA Method 6020B
Client ID: DU3-22-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-31
Date Analyzed: 08/18/21 Data File: 108248-31.135
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 9.46
Lead 18.2
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
35
Analysis For Total Metals By EPA Method 6020B
Client ID: DU4-5-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-32
Date Analyzed: 08/18/21 Data File: 108248-32.136
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.81
Lead 29.8
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
36
Analysis For Total Metals By EPA Method 6020B
Client ID: DU4-4-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-33
Date Analyzed: 08/18/21 Data File: 108248-33.137
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.73
Lead 8.10
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
37
Analysis For Total Metals By EPA Method 6020B
Client ID: DU4-4-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-34
Date Analyzed: 08/18/21 Data File: 108248-34.138
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.50
Lead 4.95
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
38
Analysis For Total Metals By EPA Method 6020B
Client ID: DU4-3-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-35
Date Analyzed: 08/18/21 Data File: 108248-35.139
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 28.6
Lead 43.0
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
39
Analysis For Total Metals By EPA Method 6020B
Client ID: DU4-2-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-36
Date Analyzed: 08/18/21 Data File: 108248-36.140
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 10.4
Lead 34.4
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
40
Analysis For Total Metals By EPA Method 6020B
Client ID: DU4-1-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-37
Date Analyzed: 08/18/21 Data File: 108248-37.141
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 10.4
Lead 21.3
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
41
Analysis For Total Metals By EPA Method 6020B
Client ID: DU4-6-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-38
Date Analyzed: 08/18/21 Data File: 108248-38.142
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 9.79
Lead 20.1
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
42
Analysis For Total Metals By EPA Method 6020B
Client ID: DU4-6-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-39
Date Analyzed: 08/18/21 Data File: 108248-39.146
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 12.9
Lead 20.9
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
43
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-1-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-40
Date Analyzed: 08/18/21 Data File: 108248-40.147
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.16
Lead 3.26
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
44
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-2-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-41
Date Analyzed: 08/19/21 Data File: 108248-41.283
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 1.60
Lead 2.69
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
45
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-3-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-42
Date Analyzed: 08/19/21 Data File: 108248-42.244
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.12
Lead 2.89
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
46
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-3-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-43
Date Analyzed: 08/19/21 Data File: 108248-43.245
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 1.95
Lead 2.78
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
47
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-4-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-44
Date Analyzed: 08/19/21 Data File: 108248-44.246
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.29
Lead 3.79
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
48
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-5-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-45
Date Analyzed: 08/19/21 Data File: 108248-45.247
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 1.46
Lead 2.90
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
49
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-6-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-46
Date Analyzed: 08/19/21 Data File: 108248-46.248
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 1.87
Lead 2.69
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
50
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-7-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-47
Date Analyzed: 08/19/21 Data File: 108248-47.286
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.60
Lead 7.42
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
51
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-7-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-48
Date Analyzed: 08/19/21 Data File: 108248-48.287
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.05
Lead 4.94
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
52
Analysis For Total Metals By EPA Method 6020B
Client ID: DU6-8-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-49
Date Analyzed: 08/19/21 Data File: 108248-49.290
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.54
Lead 10.4
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
53
Analysis For Total Metals By EPA Method 6020B
Client ID: DU5-1-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-50
Date Analyzed: 08/19/21 Data File: 108248-50.291
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 5.14
Lead 12.2
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
54
Analysis For Total Metals By EPA Method 6020B
Client ID: DU5-2-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-51
Date Analyzed: 08/19/21 Data File: 108248-51.292
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.36
Lead 10.7
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
55
Analysis For Total Metals By EPA Method 6020B
Client ID: DU5-3-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-52
Date Analyzed: 08/19/21 Data File: 108248-52.293
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.14
Lead 2.77
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
56
Analysis For Total Metals By EPA Method 6020B
Client ID: DU5-4-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-53
Date Analyzed: 08/19/21 Data File: 108248-53.294
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.26
Lead 3.63
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
57
Analysis For Total Metals By EPA Method 6020B
Client ID: DU5-5-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-54
Date Analyzed: 08/19/21 Data File: 108248-54.297
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.61
Lead 5.40
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
58
Analysis For Total Metals By EPA Method 6020B
Client ID: DU5-6-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-55
Date Analyzed: 08/19/21 Data File: 108248-55.298
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.32
Lead 5.80
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
59
Analysis For Total Metals By EPA Method 6020B
Client ID: DU5-7-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-56
Date Analyzed: 08/19/21 Data File: 108248-56.299
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.47
Lead 5.82
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
60
Analysis For Total Metals By EPA Method 6020B
Client ID: DU5-4-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-57
Date Analyzed: 08/19/21 Data File: 108248-57.300
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.15
Lead 5.44
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
61
Analysis For Total Metals By EPA Method 6020B
Client ID: DU2-1-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-58
Date Analyzed: 08/19/21 Data File: 108248-58.301
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.22
Lead 7.59
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
62
Analysis For Total Metals By EPA Method 6020B
Client ID: DU2-1-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-59
Date Analyzed: 08/19/21 Data File: 108248-59.302
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.58
Lead 5.06
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
63
Analysis For Total Metals By EPA Method 6020B
Client ID: DU2-2-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-60
Date Analyzed: 08/19/21 Data File: 108248-60.303
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.65
Lead 7.13
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
64
Analysis For Total Metals By EPA Method 6020B
Client ID: DU2-3-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-61
Date Analyzed: 08/19/21 Data File: 108248-61.309
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.19
Lead 6.78
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
65
Analysis For Total Metals By EPA Method 6020B
Client ID: DU2-4-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-62
Date Analyzed: 08/19/21 Data File: 108248-62.304
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.56
Lead 7.21
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
66
Analysis For Total Metals By EPA Method 6020B
Client ID: DU2-5-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-63
Date Analyzed: 08/19/21 Data File: 108248-63.305
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.28
Lead 4.58
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
67
Analysis For Total Metals By EPA Method 6020B
Client ID: DU2-5-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-64
Date Analyzed: 08/19/21 Data File: 108248-64.306
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.51
Lead 3.99
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
68
Analysis For Total Metals By EPA Method 6020B
Client ID: DU2-6-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-65
Date Analyzed: 08/19/21 Data File: 108248-65.312
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 1.98
Lead 6.22
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
69
Analysis For Total Metals By EPA Method 6020B
Client ID: DU2-7-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-66
Date Analyzed: 08/19/21 Data File: 108248-66.313
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.04
Lead 6.52
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
70
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-1-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-67
Date Analyzed: 08/19/21 Data File: 108248-67.314
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 5.49
Lead 12.2
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
71
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-2-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-68
Date Analyzed: 08/19/21 Data File: 108248-68.315
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 7.70
Lead 19.8
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
72
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-3-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-69
Date Analyzed: 08/19/21 Data File: 108248-69.316
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 15.0
Lead 28.5
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
73
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-4-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-70
Date Analyzed: 08/19/21 Data File: 108248-70.317
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 7.58
Lead 33.8
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
74
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-4-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-71
Date Analyzed: 08/19/21 Data File: 108248-71.318
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 7.56
Lead 17.2
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
75
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-5-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-72
Date Analyzed: 08/19/21 Data File: 108248-72.321
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 6.96
Lead 18.3
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
76
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-6-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-73
Date Analyzed: 08/19/21 Data File: 108248-73.322
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.65
Lead 8.84
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
77
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-7-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-74
Date Analyzed: 08/19/21 Data File: 108248-74.323
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 9.20
Lead 18.8
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
78
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-8-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-75
Date Analyzed: 08/19/21 Data File: 108248-75.324
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 12.4
Lead 19.0
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
79
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-9-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-76
Date Analyzed: 08/19/21 Data File: 108248-76.325
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 8.58
Lead 10.6
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
80
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-10-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-77
Date Analyzed: 08/19/21 Data File: 108248-77.326
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 7.07
Lead 7.51
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
81
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-11-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-78
Date Analyzed: 08/19/21 Data File: 108248-78.327
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.63
Lead 4.31
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
82
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-12-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-79
Date Analyzed: 08/19/21 Data File: 108248-79.328
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 4.74
Lead 4.35
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
83
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-12-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-80
Date Analyzed: 08/19/21 Data File: 108248-80.329
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.20
Lead 4.36
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
84
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-13-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-81
Date Analyzed: 08/19/21 Data File: 108248-81.243
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 8.80
Lead 11.8
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
85
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-19-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-82
Date Analyzed: 08/19/21 Data File: 108248-82.335
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 6.17
Lead 4.56
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
86
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-15-6 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-83
Date Analyzed: 08/19/21 Data File: 108248-83.336
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 3.45
Lead 6.89
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
87
Analysis For Total Metals By EPA Method 6020B
Client ID: DU1-15-12 Client: PBS Engineering and Environmental
Date Received: 08/16/21 Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: 108248-84
Date Analyzed: 08/19/21 Data File: 108248-84.337
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic 2.86
Lead 3.54
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
88
Analysis For Total Metals By EPA Method 6020B
Client ID: Method Blank Client: PBS Engineering and Environmental
Date Received: Not Applicable Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: I1-506 mb
Date Analyzed: 08/18/21 Data File: I1-506 mb.041
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic <1
Lead <1
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
89
Analysis For Total Metals By EPA Method 6020B
Client ID: Method Blank Client: PBS Engineering and Environmental
Date Received: Not Applicable Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: I1-507 mb
Date Analyzed: 08/18/21 Data File: I1-507 mb.049
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic <1
Lead <1
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
90
Analysis For Total Metals By EPA Method 6020B
Client ID: Method Blank Client: PBS Engineering and Environmental
Date Received: Not Applicable Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: I1-508 mb
Date Analyzed: 08/18/21 Data File: I1-508 mb.081
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic <1
Lead <1
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
91
Analysis For Total Metals By EPA Method 6020B
Client ID: Method Blank Client: PBS Engineering and Environmental
Date Received: Not Applicable Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: I1-509 mb
Date Analyzed: 08/18/21 Data File: I1-509 mb.087
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic <1
Lead <1
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
92
Analysis For Total Metals By EPA Method 6020B
Client ID: Method Blank Client: PBS Engineering and Environmental
Date Received: Not Applicable Project: 41515.009, F&BI 108248
Date Extracted: 08/18/21 Lab ID: I1-510 mb
Date Analyzed: 08/18/21 Data File: I1-510 mb.089
Matrix: Soil Instrument: ICPMS2
Units: mg/kg (ppm) Dry Weight Operator: AP
Concentration
Analyte: mg/kg (ppm)
Arsenic <1
Lead <1
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
93
Date of Report: 08/23/21
Date Received: 08/16/21
Project: Illahee MS Soil Sampling 41515.009, F&BI 108248
QUALITY ASSURANCE RESULTS
FOR THE ANALYSIS OF SOIL SAMPLES
FOR TOTAL METALS USING EPA METHOD 6020B
Laboratory Code: 108248-01 (Matrix Spike)
Analyte
Reporting
Units
Spike
Level
Sample
Result
(Wet wt)
Percent
Recovery
MS
Percent
Recovery
MSD
Acceptance
Criteria
RPD
(Limit 20)
Arsenic mg/kg (ppm) 10 6.45 80 88 75-125 10
Lead mg/kg (ppm) 50 24.9 82 85 75-125 4
Laboratory Code: Laboratory Control Sample
Analyte
Reporting
Units
Spike
Level
Percent
Recovery
LCS
Acceptance
Criteria
Arsenic mg/kg (ppm) 10 97 80-120
Lead mg/kg (ppm) 50 94 80-120
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
94
Date of Report: 08/23/21
Date Received: 08/16/21
Project: Illahee MS Soil Sampling 41515.009, F&BI 108248
QUALITY ASSURANCE RESULTS
FOR THE ANALYSIS OF SOIL SAMPLES
FOR TOTAL METALS USING EPA METHOD 6020B
Laboratory Code: 108248-21 (Matrix Spike)
Analyte
Reporting
Units
Spike
Level
Sample
Result
(Wet wt)
Percent
Recovery
MS
Percent
Recovery
MSD
Acceptance
Criteria
RPD
(Limit 20)
Arsenic mg/kg (ppm) 10 2.72 95 105 75-125 10
Lead mg/kg (ppm) 50 7.46 93 98 75-125 5
Laboratory Code: Laboratory Control Sample
Analyte
Reporting
Units
Spike
Level
Percent
Recovery
LCS
Acceptance
Criteria
Arsenic mg/kg (ppm) 10 97 80-120
Lead mg/kg (ppm) 50 96 80-120
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
95
Date of Report: 08/23/21
Date Received: 08/16/21
Project: Illahee MS Soil Sampling 41515.009, F&BI 108248
QUALITY ASSURANCE RESULTS
FOR THE ANALYSIS OF SOIL SAMPLES
FOR TOTAL METALS USING EPA METHOD 6020B
Laboratory Code: 108248-41 (Matrix Spike)
Analyte
Reporting
Units
Spike
Level
Sample
Result
(Wet wt)
Percent
Recovery
MS
Percent
Recovery
MSD
Acceptance
Criteria
RPD
(Limit 20)
Arsenic mg/kg (ppm) 10 1.52 94 98 75-125 4
Lead mg/kg (ppm) 50 2.56 90 95 75-125 5
Laboratory Code: Laboratory Control Sample
Analyte
Reporting
Units
Spike
Level
Percent
Recovery
LCS
Acceptance
Criteria
Arsenic mg/kg (ppm) 10 98 80-120
Lead mg/kg (ppm) 50 101 80-120
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
96
Date of Report: 08/23/21
Date Received: 08/16/21
Project: Illahee MS Soil Sampling 41515.009, F&BI 108248
QUALITY ASSURANCE RESULTS
FOR THE ANALYSIS OF SOIL SAMPLES
FOR TOTAL METALS USING EPA METHOD 6020B
Laboratory Code: 108248-61 (Matrix Spike)
Analyte
Reporting
Units
Spike
Level
Sample
Result
(Wet wt)
Percent
Recovery
MS
Percent
Recovery
MSD
Acceptance
Criteria
RPD
(Limit 20)
Arsenic mg/kg (ppm) 10 2.04 99 103 75-125 4
Lead mg/kg (ppm) 50 6.31 94 95 75-125 1
Laboratory Code: Laboratory Control Sample
Analyte
Reporting
Units
Spike
Level
Percent
Recovery
LCS
Acceptance
Criteria
Arsenic mg/kg (ppm) 10 96 80-120
Lead mg/kg (ppm) 50 99 80-120
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
97
Date of Report: 08/23/21
Date Received: 08/16/21
Project: Illahee MS Soil Sampling 41515.009, F&BI 108248
QUALITY ASSURANCE RESULTS
FOR THE ANALYSIS OF SOIL SAMPLES
FOR TOTAL METALS USING EPA METHOD 6020B
Laboratory Code: 108248-81 x5 (Matrix Spike)
Analyte
Reporting
Units
Spike
Level
Sample
Result
(Wet wt)
Percent
Recovery
MS
Percent
Recovery
MSD
Acceptance
Criteria
RPD
(Limit 20)
Arsenic mg/kg (ppm) 10 7.76 96 85 75-125 12
Lead mg/kg (ppm) 50 11.2 97 89 75-125 9
Laboratory Code: Laboratory Control Sample
Analyte
Reporting
Units
Spike
Level
Percent
Recovery
LCS
Acceptance
Criteria
Arsenic mg/kg (ppm) 10 93 80-120
Lead mg/kg (ppm) 50 95 80-120
FRIEDMAN & BRUYA, INC.
_________________________________________________
ENVIRONMENTAL CHEMISTS
98
Data Qualifiers & Definitions a - The analyte was detected at a level less than five times the reporting limit. The RPD results may not provide reliable information on the variability of the analysis.
b - The analyte was spiked at a level that was less than five times that present in the sample. Matrix spike recoveries may not be meaningful.
ca - The calibration results for the analyte were outside of acceptance criteria. The value reported is an estimate.
c - The presence of the analyte may be due to carryover from previous sample injections.
cf - The sample was centrifuged prior to analysis.
d - The sample was diluted. Detection limits were raised and surrogate recoveries may not be meaningful.
dv - Insufficient sample volume was available to achieve normal reporting limits.
f - The sample was laboratory filtered prior to analysis.
fb - The analyte was detected in the method blank.
fc - The analyte is a common laboratory and field contaminant.
hr - The sample and duplicate were reextracted and reanalyzed. RPD results were still outside of control limits. Variability is attributed to sample inhomogeneity.
hs - Headspace was present in the container used for analysis.
ht – The analysis was performed outside the method or client-specified holding time requirement.
ip - Recovery fell outside of control limits due to sample matrix effects.
j - The analyte concentration is reported below the lowest calibration standard. The value reported is an estimate.
J - The internal standard associated with the analyte is out of control limits. The reported concentration is an estimate.
jl - The laboratory control sample(s) percent recovery and/or RPD were out of control limits. The reported concentration should be considered an estimate. js - The surrogate associated with the analyte is out of control limits. The reported concentration should be considered an estimate.
lc - The presence of the analyte is likely due to laboratory contamination.
L - The reported concentration was generated from a library search.
nm - The analyte was not detected in one or more of the duplicate analyses. Therefore, calculation of the RPD is not applicable.
pc - The sample was received with incorrect preservation or in a container not approved by the method. The value reported should be considered an estimate. ve - The analyte response exceeded the valid instrument calibration range. The value reported is an estimate.
vo - The value reported fell outside the control limits established for this analyte.
x - The sample chromatographic pattern does not resemble the fuel standard used for quantitation.
